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Effect of Sintering Aid on Synthesis and Magnetic Properties of Nanocrystalline BaFe12O19 Ceramic Foam
Abstract:
BaFe12O19 ceramic foam was synthesized from the mixture of Fe2O3 and BaCO3 using polymeric sponge replication technique. Effect of 1, 1.5, 2, 2.5, and 3 wt.% of SiO2 addition on foam lattice shape and magnetic properties of foams were investigated. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), vibrating samplemagnetometer (VSM) and Brunauer–Emmett–Teller (BET) techniques.Addition of 3 wt.% SiO2 can completely maintain the foam lattice shape at lower calcination temperature of 1075 °C. It resulted in higher values of coercivity and saturation magnetization. Moreover, BET analysis of the foam sample with 3 wt.% SiO2 demonstrate a specific surface area of 0.3 m2g-1.
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980-984
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December 2012
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© 2013 Trans Tech Publications Ltd. All Rights Reserved
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