Effect of Composition and Thermo-Mechanical Processing on Microstructure Development in Ni-30Fe-Nb-C Model Alloys

Article Preview

Abstract:

The unavoidable phase transformation upon cooling makes a direct observation of austenite microstructure impossible. One of the methods to investigate the high temperature condition of austenite is to use a model alloy, which would not transform to martensite on quenching. In the present work the recrystallisation and grain growth of austenite during thermo-mechanical processing (TMP) were studied for three Ni-30Fe-Nb-C alloys containing 0.33, 0.85 and 1.42 wt% Nb. The austenite microstructures were characterised using optical and scanning electron microscopy, and energy dispersive X-ray spectroscopy. The austenite recrystallisation kinetics was investigated with respect to the precipitate distribution variations. A relative strength of the grain boundary pinning effect from solute Nb and precipitated particles is discussed.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

475-480

Citation:

Online since:

May 2014

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2014 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] G.E. Dieter, Mechanical Metallurgy, McGraw-Hill Book Company, London, (1998).

Google Scholar

[2] P.J. Hurley, P.D. Hodgson, B.C. Muddle, A study of deformation substructures in austenite using a model Ni-30 wt. % Fe alloy, Scripta Materialia, 45 (2001) 25-32.

DOI: 10.1016/s1359-6462(01)00987-3

Google Scholar

[3] A.S. Taylor, P. Cizek and P.D. Hodgson, Comparison of 304 stainless and Ni-30 wt% Fe as potential model alloys to study the behaviour of austenite during thermomechanical processing, Acta Materialia, 59 (2011) 5832-5844.

DOI: 10.1016/j.actamat.2011.05.060

Google Scholar

[4] H. Beladi, P. Cizek and P.D. Hodgson, New insight into the mechanism of metadynamic softening in austenite, Acta Materialia, 59 (2011) 1482-1492.

DOI: 10.1016/j.actamat.2010.11.012

Google Scholar

[5] O. Kwon, A.J. DeArdo, Interactions between recrystallization and precipitation in hot-deformed microalloyed steels, Acta Metallurgica et Materiealia 39(4) (1991) 529 - 538.

DOI: 10.1016/0956-7151(91)90121-g

Google Scholar

[6] H.S. Zurob, G. Zhu, S.V. Subramanian, G.R. Purdy, C.R. Hutchinson and Y. Brechet, Analysis of the effect of Mn on the recrystallization kinetics of high Nb steel: an example of physically-based alloy design, ISIJ Int. 45(5) (2005) 713 - 722.

DOI: 10.2355/isijinternational.45.713

Google Scholar

[7] C.R. Hutchinson, H.S. Zurob, C.W. Sinclair and Y.J.M. Brechet, The comparative effectiveness of Nb solute and NbC precipitates at impeding grain-boundary motion in Nb steels, Scripta Materialia, 59 (2008) 635 - 637.

DOI: 10.1016/j.scriptamat.2008.05.036

Google Scholar

[8] S. Vervynckt, K. Verbeken, P. Thibaux, Y. Houbaert, Recrystallization–precipitation interaction during austenite hot deformation of a Nb microalloyed steel, Materials Science and Engineering A 528 (2011) 5519 - 5528.

DOI: 10.1016/j.msea.2011.03.087

Google Scholar

[9] C.L. Miao, C.J. Shang, H.S. Zurob, G.D. Zhang, and S.V. Subramanian, Recrystallization, precipitation behaviors, and refinement of austenite grains in high Mn, high Nb steel, Metallurgical and Materials Transactions A 43 (2012) 665 - 676.

DOI: 10.1007/s11661-011-0895-5

Google Scholar

[10] B. Feng, Effect of Ti and Ti-Nb on the stability of the austenite grain structure and austenite to ferrite transformation characteristics in C-Mn steel under hot rolling conditions, PhD Thesis, University of Wollongong, (1991).

Google Scholar

[11] R. P. de Siqueira, H. R. Z. Sandim and D. Raabe, Particle stimulated nucleation in coarse-grained ferritic stainless steel, Metallurgical and Materials Transactions A, 44 (2013) 469 – 478.

DOI: 10.1007/s11661-012-1408-x

Google Scholar

[12] H.S. Zurob, Effects of precipitation, recovery and recrystallization on the microstructural evolution of the microalloyed austenite, PhD Thesis, McMaster University, (2003).

Google Scholar

[13] T. Gladman, The Physical Metallurgy of Microalloyed Steels, The Institute of Materials, London, (1997).

Google Scholar

[14] A.J. DeArdo, Niobium in modern steels, International Materials Reviews, 48(6) (2003) 371 - 402.

DOI: 10.1179/095066003225008833

Google Scholar