Controlled Macrostepping of Si-Face 4°off 4H-SiC over a Large Area via Liquid Si-Induced Reconstruction

Article Preview

Abstract:

The reconstruction of 4°off 4H-SiC surfaces was investigated using Si melting at 1550°C in a SiC/Si/SiC sandwich configuration. Despite systematically obtaining a macrostepped morphology over the entire areas in contact with the liquid Si, the steps were found wavy when using as-received 4H-SiC wafers. The regularity and straightness of the steps were significantly improved when the surface reconstruction was performed on processed surfaces: on re-polished surfaces the steps were found to be regular and straight in some cases, while this was constantly observed on as-grown epitaxial layers. After a reconstruction process of 2h, the best regularity of the steps was obtained with an average width of ̴ 3-5 μm. Increasing the processed area from 1.44 to 4 cm2 did not affect the results which suggests a good scalability of the process.

You might also be interested in these eBooks

Info:

* - Corresponding Author

[1] J. Woerle, B. C. Johnson, C. Bongiorno, K. Yamasue, G. Ferro, D. Dutta, T. A. Jung, H. Sigg, Y. Cho, U. Grossner, and M. Camarda, Phys. Rev. Mater., 3, 8, (2019), 084602

Google Scholar

[2] M. Camarda, J. Woerle, V. Souliere, G. Ferro, H. Sigg, U. Grossner, and J. Gobrecht, Mater. Sci. Forum, 897, (2017), 107–110

DOI: 10.4028/www.scientific.net/msf.897.107

Google Scholar

[3] V. Soulière, D. Carole, M. Camarda, J. Woerle, U. Grossner, O. Dezellus, and G. Ferro, Mater. Sci. Forum, 858, (2016), 163–166

DOI: 10.4028/www.scientific.net/msf.858.163

Google Scholar

[4] X. Xing, T. Yoshikawa, O. Budenkova, and D. Chaussende, J. Mater. Sci., 57, 2, (2022), 972–982

Google Scholar

[5] Y. Jousseaume, F. Cauwet, and G. Ferro, Mater. Sci. Forum, 1062, (2022), 8–12

Google Scholar

[6] Y. Jousseaume, F. Cauwet and G. Ferro, Poster presentation at ICSCRM2022 (session Tu-P-B)

Google Scholar

[7] Y. Jousseaume, F. Cauwet and G. Ferro, J. Cryst. Growth, 593, (2022), 126783

Google Scholar

[8] K. Alassaad, V. Soulière, F. Cauwet, H. Peyre, D. Carole, P. Kwasnicki, S. Juillaguet, T. Kups, J. Pezoldt and G. Ferro, Acta Materialia, 75, (2014), 219–226

DOI: 10.1016/j.actamat.2014.04.057

Google Scholar