Analysis of Dislocations Nucleated after Nano Indentation Tests at Room Temperature in 4H-SiC

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Abstract:

4H-SiC intrinsic homoepitaxied single crystals have been nano indented at room temperature using a spherical indentor and the related deformation microstructures have been analyzed by Transmission Electron Microscopy. Dislocations are lying in the basal plane but have been found to be perfect, in contrast with observations made at higher temperature. Although such a change in deformation mechanism has been observed in other semiconductors such as Silicon and Indium Antimonide, it was unexpected in a very low stacking fault material such as SiC.

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Materials Science Forum (Volumes 717-720)

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339-342

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May 2012

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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[1] P. Pirouz, M. Zhang, J.L. Demenet and H.M. Hobgood, Transition from brittleness to ductility in SiC, J. Phys.: Condens. Matter 14 (2002) 12929-12945.

DOI: 10.1088/0953-8984/14/48/335

Google Scholar

[2] P. Pirouz, J.L. Demenet and M.H. Hong, On transition temperatures in the plasticity and fracture of semiconductors, Phil. Mag. A 81 (2001) 1207-1227.

DOI: 10.1080/01418610108214437

Google Scholar

[3] A. Mussi, J. Rabier, L. Thilly and J.L. Demenet, Plasticity and deformation microstructure of 4H-SiC below the brittle-to-ductile transition, phys. stat. sol. (c) 4 (2007) 2929-2933.

DOI: 10.1002/pssc.200675438

Google Scholar

[4] J.L. Demenet, X. Milhet and J. Rabier, TEM observations of the coexistence of perfect and dissociated dislocations in SiC under high stress, phys. stat. sol. (c) 202 (2005) 1987-1991.

DOI: 10.1002/pssc.200460541

Google Scholar

[5] D. Cherns, A.R. Preston, Convergent beam diffraction studies of interfaces, defects, and multilayers, J. Electr. Microsc. Tech. 13 (1989) 111-122.

DOI: 10.1002/jemt.1060130204

Google Scholar

[6] J.L. Demenet, M. Amer, C. Tromas and J. Rabier, to be published.

Google Scholar

[7] T.F. Page, L. Riester, S.V. Hainsworth, The plasticity response of 6H-SiC and related materials to nanoindentation: slip vs densification, Mater. Res. Soc. Symp. Proc. 522 (1998) 113-118.

DOI: 10.1557/proc-522-113

Google Scholar

[8] J. Rabier and J.L. Demenet, Low temperature, high stress plastic deformation of semiconductors: the silicon case, phys. stat. sol. (b) 222 (2000) 63-74.

DOI: 10.1002/1521-3951(200011)222:1<63::aid-pssb63>3.0.co;2-e

Google Scholar

[9] B. Kedjar, L. Thilly, J.L. Demenet, J. Rabier, Plasticity of indium antimonide between -176°C and 400°C under hydrostatic pressure. Part II: Microscopic aspects of the deformation, Acta Mater. 58 (2010) 1426-1440.

DOI: 10.1016/j.actamat.2009.10.052

Google Scholar

[10] M.H. Hong, A.V. Samant, and P. Pirouz, Stacking fault energy of 6H-SiC and 4H-SiC single crystals, Phil. Mag. A 80 (2000) 919-935.

DOI: 10.1080/014186100250615

Google Scholar

[11] K. Maeda, K. Suzuki, S. Fujita, M. Ichihara and S. Hyodo, Defects in plastically deformed 6H-SiC single crystals studied by transmission electron microscopy, Phil. Mag. A 57 (1988) 573-592.

DOI: 10.1080/01418618808214408

Google Scholar

[12] A. Mussi, J.L. Demenet and J. Rabier, TEM study of defects generated in 4H-SiC by microindentations on the prismatic plane, Phil. Mag. Lett. 86 (2006) 561-568.

DOI: 10.1080/09500830600930198

Google Scholar