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HomeMaterials Science ForumMaterials Science Forum Vol. 898Effect of Molten NaCl on the Synthesis of Ti3SiC2...

Effect of Molten NaCl on the Synthesis of Ti₃SiC₂ Powders

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Abstract:

Free Ti/Si/C powder mixtures with or without molten salt were heated under vacuum with various schedules. The effect of molten salt during synthesis on the morphology and phase composition of Ti₃SiC₂ powders were investigated. The combustion powders were analyzed by DSC, XRD, SEM and EDS. The results indicated that the existence of molten salt could promote the reaction process and decrease the synthesis temperature. The Ti₃SiC₂ powders obtained by molten salt method were uniform and well dispersive. The content of Ti₃SiC₂ phase was influenced by salt/powders ratio and molding pressure. The appropriate salt/powders ratio and pre-press pressure were 1:1and 100 MPa, respectively.

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IUMRS International Conference in Asia

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Periodical:

Materials Science Forum (Volume 898)

Pages:

1611-1616

DOI:

https://doi.org/10.4028/www.scientific.net/MSF.898.1611

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Online since:

June 2017

Authors:

Xue Guo, Jun Xia Wang, Shi Yuan Yang, Yu Run Feng, Hong Yu Gong, Yu Jun Zhang*

Keywords:

Agglomeration, Ceramics, Microstructure, Molten Salt, Powder, Ti₃SiC₂

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© 2017 Trans Tech Publications Ltd. All Rights Reserved

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