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HomeMaterials Science ForumMaterials Science Forum Vol. 944Micromorphology and Characterization of V2O3...

Micromorphology and Characterization of V₂O₃ Nanoparticles Produced by the Liquid Phase Reduction-Heat Treatment

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Abstract:

The liquid phase reduction-heat treatment has been used to prepare V₂O₃ nanoparticles in this paper. It is a novel method that the precursor was developed by Oxalic acid dehydrate (H₂C₂O₄·2H₂O) reduction of V₂O₅ powder in anhydrous ethanol. V₂O₃ nanoparticles were successfully obtained by thermal treatment of the precursor. The phase, composition, structure, and morphology of the as-obtained samples were verified by XRD, XPS, SEM and TEM measurements. Meanwhile, the possible formation mechanism of V₂O₃ in the heat-treatment is briefly discussed by analyzing the DSC.

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Functional and Functionally Structured Materials III

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Materials Science Forum (Volume 944)

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650-656

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https://doi.org/10.4028/www.scientific.net/MSF.944.650

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January 2019

Authors:

Ming Rui Zhang, Yuan Qin, Dao Zhang, Guang Yuan Wang, Sen Yang*

Keywords:

Liquid Phase Reduction, Thermal Reduction, V₂O₃ Nanoparticles

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