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Mechanochemical synthesis occurs at the boundaries of continually regenerating, nanometre-sized grains and allows chemical reactions to proceed at low temperatures in a ball mill without external heating [26].
These peaks indicated the existence of the crystalline spinel-structured magnetite (Fe3O4) phase of iron oxide, which corresponds to JCPDS number 19-629 [55].

., which involve a number of systematic errors in the measurement of θ and hence d values.
A general increase in impedance may be due to increases in the band gap of the nanocrystalline films, and due to decreases in grain size by increasing the composition parameter ‘x’. 6.5.

Failure to treat diabetes effectively, will largely result into a number of other health complications, such as eye problems (blindness), neuropathy, foot complications, kidney disease, heart diseases, hypertension, stroke, hyperglycemic nonketonic syndrome, gastroparesis, heart disease, and mental health disorders; death and disability in the entire globe, it may also affect pregnancy [1, 2].
XRD Analysis The phase variety and grain size of synthesized silver nanoparticles was determined by X-ray diffraction Spectroscopy (Philips PAN analytical).

By 2050, this number is expected to rise to 10 million if nothing is done [3].
Chitkara, Morphological analysis and grain size distribution of SnO2 nanoparticles via digital image processing across diverse calcination temperatures, J.

Treatments for precision fiber cleaning may be utilized to eliminate impurities and starch grains [30].
Siddique, Optimum process parameters selection for Brinell hardness number of natural fiber reinforced composites using Taguchi method, Saudi J.

The geology of the Djerid Chott basin was discussed by a number of authors [33-34].
Yaich, Cyclicity of grain size parameters along a Core from the Gleysol of Sebkha Ennoual, southeastern Tunisia, J. basic appl. res. (2015) 124-134

The abbe refractometer has an accuracy of 0.0002, with the fourth decimal place determined by averaging a large number of individual measurements.
The TEM analysis technique was used to determine the nanoparticle size, crystallite size, grain size measurement, and atomic arrangement of the nanoparticles.

Contrariwise, a low energy input at fast scan speed is accompanied by another type of porosity defect, “lack of fusion” (LOF), where we notice no melted grains on the powder bed surface (Fig. 2c).
In fact, a various number of research studies do not consider radiation effect owing to the small melt pool dimension in comparison with the whole simulation domain [22].

Difficulties during those operations are stipulated by the fact that the mass enclosing the coal seam contains the rocks with low water yield – water-bearing, fine-grained, and argillaceous sands [12].
Certain number of sections near western technical limits was not mined.

The summary of the coating deposition parameters of both nano and conventional coating is given below in Table 2 and 3: Table 2: Summary of nano coating deposition parameters Machine used Standard Balzers rapid coating system (RCS) machine Make Oerlikon Balzers, Swiss Targets composition For TiAlN coating: Ti, Ti50Al50 Number of targets Ti(02), Ti50Al50 (04) Targets power 3.5 kW Reactive gas Nitrogen Nitrogen deposition pressure 3.5 pa Substrate bias voltage -40V to -170V Substrate temperature 450°C±10°C Coating Thickness 4µm±1µm Table 3: Summary of conventional coating deposition parameters Arc Current (A) 750 Arc Voltage (V) 45 Powder Feed Rate (rev/min) 5.2 Spraying Distance (mm) 90-110 Plasma Arc Gas (Argon) Pressure 58 psi Powder Gas Pressure 60 psi AUX Gas Pressure 10 psi Characterization of Coating The coatings were characterised with relative to the parameters affecting the behaviour of coatings for high temperature applications.
In case of conventional TiAlN coatings having higher grain size as well as pores, so at higher speed the large amplitudes of dimensional variation cause wear rate from the third body action especially when loose wear particles slide and roll between mating surfaces.