Advanced Materials Research Vol. 1133

Abstract: A conventional tube is considered in oblique position when its longitudinal is oblique. However, oblique attachments vary as the tube can be a straight or angulated tube. In the present study, impact responses of different oblique positioned tubes subject to axial loading were numerically studied. Next, the best oblique arrangements were proposed that have higher critical load angle and energy absorption capacity. Results show that specimen of Top-Bottom Angulated (TBA) from horizontal is the best choice for its lowest initial peak load and mean crush load. This data therefore has great potential for further enhance the new design of energy absorbers in oblique position.

Abstract: Cobalt chromium molybdenum (CoCrMo) alloy is widely used in artificial hip and knee joints because of their excellence corrosion and wear resistance, as well as good mechanical properties and biocompatibility. This study investigates the effect of sintering temperature on the microstructure and mechanical properties of CoCrMo using powder metallurgy technique. CoCrMo powder was mixed with zinc stearate and then put into the shaker mixer at 65 rpm for 3 hours. The powder was then compacted at a pressure of 18T using an automated hydraulic press and sintered at a temperature in the range of 1200 – 1400 °C under 95 Vol% N₂/ 5 Vol% H₂ atmosphere. The microstructure, physical and mechanical properties of the samples are analyzed using scanning electron microscopy (SEM), Vickers’s microhardness tester and transverse rupture strength (TRS). The study reveals that the density, hardness and strength of CoCrMo samples increase as sintering temperature increases.

Abstract: This paper presents the alloyability of FeCrCu powder compacts formed through warm powder compaction route. A lab-scale uni-axial die compaction rig was designed and fabricated which enabled the powder forming at elevated temperature. Iron powder ASC 100.29 was mechanically mixed with other alloying elements, i.e., copper (Cu) and chromium (Cr) as well as carbon (C) as additive for 60 minutes. Green samples were formed at 30°C (room temperature), 100°C, and 180°C through simultaneous upward and downward axial loadings. The defect-free green compacts were subsequently sintered in argon gas fired furnace at 900°C and 1000°C for 60 minutes at a rate of 5°C/minute. The alloyability of the sintered products was analyzed through XRD testing. The compressive strength of the sintered samples was also measured. The results revealed that FeCrCu alloy was formed at different intensity depended upon the forming and sintering temperature. The compressive strength was found to be highest for sample formed at 180°C and sintered at 1000°C.

Abstract: NiTi is categorized as a Shape Memory Alloy (SMA) that has been commercially studied and used in biomedical industry due to two main unique properties, Pseudoelastic (PE) and Shape Memory Effect (SME). Combined with biomimetic properties to human bone, NiTi has the potential to be applied as implants by engineered manufacturing process. The common manufacturing by casting has some challenges in order to obtain intrinsic and miscellaneous design of NiTi parts leash to explore more using powder metallurgy (PM) method that expected to get the porous structure. This paper aims to provide an overview of processing NiTi by conventional PM method which could contribute in focusing porous part that suits for biomedical and implants.

Abstract: The demand for components manufactured by Metal Injection Molding (MIM) has been increased due to a diverse range of applications on the high temperature mechanical properties and corrosion/oxidation resistance. Super alloy utilize the inherent physical properties of heat-resisting alloy based on iron-nickel, or cobalt specifically high purity and fine particle size distributions, which can enhance sintering and maximize the density of the final component. The development of super alloy Inconel 718 (IN718) using MIM is discussed. IN718 powder with binder formulation consists of polyethylene (PE) / palm stearin (PS) were mixed homogeneously and injected to produce green compacts. The binders then were removed through solvent extraction process from various heating temperature and duration of time. The binder removal was quantified by weight loss measurements and the evolution of pore structure for the debound specimens was observed using scanning electron microscope (SEM). Result shows that complete extraction of PS from the green parts can be concluded during 60 °C of heating and 6 hours of immersion in heptane.

Abstract: Designing orthodontic implants with desired physical and biological performances and to fabricate net shape with complex anatomical shapes is still a challenge. Cautious design approaches followed by systematic manufacturing techniques that can achieve balanced physical performance in mono block implants mechanics is necessary to accomplish this objective. Metal additive manufacturing (MAM) technique such as selective laser melting (SLM) process is progressively being utilized for new biomaterials such as cobalt-chrome-molybdenum (CoCrMo). This study was designed to determine a dimensional accuracy of open cellular structures CoCrMo samples with designing volume based porosity ranging between 0 % (full dense) to 80 %. A maximum 2.10 % shrinkage was obtained by 80 % designed porosity sample. Samples with higher volume-to-surface area (full dense) demonstrated the low total amount of shrinkage as compared to lower volume-to-surface area (80 % designed porosity).

Abstract: CoCrMo alloy is one of the most used metallic biomaterials due to its high wear. Premature wear of the component is one of the main cause of hip prosthesis failure. The objective in this study is to investigate the tribology properties of sintered CoCrMo fabricated via injection moulding. Tests were carried out at room temperature comparing metal injection moulded dog bone tensile samples at different sintering temperatures. The parameter used for the pin on disk test is a 10kN load, 500m sliding distance and a chromium steel ball as a sliding partner. The morphologies and compositions of the worn surfaces were analysed by optical and scanning electron microscope. The results showed that the wear mechanism and friction coefficient of CoCrMo depended strongly on the microstructure which was influenced by the sintering temperature.

Abstract: Feedstock preparation is one of the most crucial steps that will influence the metal injection molding process. In this study, the properties of Cu and space holder powder were determined. Powder morphology was captured using Scanning Electron Microscopy (SEM). Three different ratios of feedstocks were premixed with potassium carbonate as space holder using Turbulence Shaker mixer prior to mixing with constant binder system consist of waste rubber (WR). Mixes of three feedstocks with from 40, 50 and 60 wt. % were carried out in Brabender Plasticoder. All feedstocks were mixed at constant powder loading. The feedstocks were successfully injection molded using Vertical Injection Molding machine at 200°C.

Abstract: In this present work, NiTi alloy has been successfully produced by metal injection moulding (MIM) starting with elemental powders mixture of Nickel (Ni) and Titanium (Ti) mixed with a composite binder of palm stearin (PS) and polyethylene (PE). Two different atomic fractions of Ni-Ti were investigated; 50-50 and 50.8-49.2 and the powder loading used was 65.5vol%. The green parts were successfully injection moulded at an optimum temperature of 130°C. The samples were then underwent solvent extraction using n-heptane solution to remove the primary binder of PS. It was followed by thermal debinding to completely remove the backbone binder of PE and subsequently sintered in high vacuum at 1050°C to allow diffusion of the elemental Ni and Ti powders to form NiTi alloy. The phase constituents of the sintered specimens were characterized by X-Ray Diffraction (XRD) and by Scanning Electron Microscopy (SEM), equipped with EDX analysis under back-scattered electron (BSE) mode. The reversible austenite to martensite phase transformation temperatures (PTTs) correspond to shape memory effect (SME) was determined by Differential Scanning Calorimeter (DSC) with heating and cooling cycle in the range of-50 and 200°C. The influence of Ni-Ti ratio and the processing conditions on phase constituents and SME was then analyzed and discussed.

Abstract: The high specific strength, ease of working, good weldability and the ability to be precipitation strengthening have increased the demand of aluminium alloys in aerospace and automobile industries. In this research the effect of artificial aging/precipitation hardening on mechanical properties and microstructures of 6061 aluminum alloy weldments produced using gas tungsten welding (TIG) was studied. The artificial aging of welded alloy was carried out at temperatures varying from 150°C to 170°C for different period of time. The Vickers hardness and tensile test were carried out to evaluate the response of material to heat treatment. The experimental work showed that the maximum hardness and tensile strength of 6061 aluminum welded samples was achieved when aged at 170°C (after solution treatment) for 2 and 10 hours. Scanning electron microstructure analysis revealed that after solution treatment, when the samples were aged at 150-170°C, the Mg₂Si precipitates present in the grains grows in size and develop stress in the grain and resulted increment in hardness.