A Study of Process Interruptions during Pre- and Post-Buffer Layer Epitaxial Growth for Defect Reduction in 4H SiC

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Abstract:

We perform epilayer growth where the process is interrupted (in situ) during post and pre buffer layer growth at a reduced temperature. Process interrupted during post buffer layer growth demonstrates significant reduction in basal plane dislocation (BPD) at a lower temperature. SIMS study demonstrates that etching takes place during the interruption time. We believe surface treatment of the buffer layer at different etching conditions during the interruption plays a major role in BPD reduction. However, the in-situ interruption, taking place prior to the buffer layer (i.e., on the substrate), does not contribute to the reduction in BPD in epilayer. We believe that the surface effect of interruption related etching on substrate during pre-buffer layer interruption, is not efficient enough to reduce BPD due to the higher doping and higher BPD associated with the substrate. Furthermore, we demonstrate that post buffer layer growth interruption contributes to the reduction in stacking faults in the epilayers. We also attribute this reduction of SF due to the surface etching prior to the drift layer growth.

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