Improvement of the Conformational Stability of 150 mm 4H SiC Wafers

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Abstract:

A method for mitigating loss of conformational stability in 150 mm n-type 4H SiC wafers was investigated. Modifications to the physical vapor transport (PVT) process used to grow the parent bulk crystals, combined with post-growth thermal treatment, were examined as means of reducing the internal stresses hypothesized to promote instability. The magnitude of the stresses was analyzed by mechanically thinning sets of wafers produced from each process to determine the critical thickness of stability loss. The average critical thickness was found to be reduced by 13% via growth cell modification, at a reduced level of thermal treatment relative to a control process, with all wafers becoming unstable greater than 30 μm below the minimum recorded production thickness. Assessment of the spatial uniformity of dislocations indicated that lower conformational stability corresponded to elevated densities of basal plane dislocations (BPDs) and threading edge dislocations (TEDs) at the wafer edge relative to the center.

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[1] R. Anzalone, N. Piluso, G. Litrico, S. Lorenti, G. Arena, S. Coffa, F. La Via, Stess relaxation mechanism after thinning process on 4H SiC substrate, Mater. Sci. Forum 924, (2018) 535-538.

DOI: 10.4028/www.scientific.net/msf.924.535

Google Scholar

[2] J. Guo, Y. Yang, B. Raghothamachar, M. Dudley, S. Stoupin, Mapping of the lattice strain in 4H-SiC crystals by synchrotron double-crystal x-ray topography, J. Electron. Mater. 47, (2018) 903-909.

DOI: 10.1007/s11664-017-5789-x

Google Scholar

[3] Y. Yang, J. Guo, B. Raghothamachar, X. Chan, T. Kim, M. Dudley, Characterization of strain due to nitrogen doping concentration variations in heavy doped 4H-SiC, J. Electron. Mater. 47, (2018) 938-943.

DOI: 10.1007/s11664-017-5846-5

Google Scholar

[4] E. Nikolova, on the Twyman effect and some of its applications, J. Materi. Sci. 20, (1985) 1-8.

Google Scholar

[5] C. Clemmow, The flexure of thick circular plates, Proc. R. Soc. Lond. A 112 (1926) 559-558.

Google Scholar

[6] I. Manning, Y. Matsuda, G. Chung, E. Sanchez, M. Dudley, T. Ailihumaer, B. Raghothamachar, Progress in bulk 4H SiC crystal growth for 150 mm wafer production, Mater. Sci. Forum 1004, (2020) 37-43.

DOI: 10.4028/www.scientific.net/msf.1004.37

Google Scholar