Non-Destructive Quantification of In-Plane Depth Distribution of Sub-Surface Damage on 4H-SiC Wafers Using Laser Light Scattering

Article Preview

Abstract:

The development of non-destructive quantitative evaluation techniques for the in-plane depth distribution of sub-surface damage (SSD) layer induced by mechanical processing of chemical mechanical polishing (CMP) finished SiC wafers is essential to reduce the occurrence of crystal defects during epitaxial growth. Until now, no wafer inspection method has been able to nondestructively and quantitatively assess the in-plane depth distribution of the SSD. This study investigates the correlation between the scattered light intensity measured nondestructively by the Laser light scattering (LLS) method and the SSD depth estimated by destructive inspection using the Dynamic AGE-ing® method, a sublimation-controlled etching and growth process, to develop a novel non-destructive SSD inspection method. As a result, it was found that there is an exponential relationship between the scattered light intensity by the LLS method on the bare wafer surface and the depth of the SSD layer that contributes to the formation of in-grown stacking faults (IGSF) during subsequent epitaxial growth. The results show that SiC wafer inspection using the novel LLS method, which introduces this relational equation, enables non-destructive and quantitative evaluation of SSD depth and in-plane distribution.

You might also be interested in these eBooks

Info:

* - Corresponding Author

[1] A. Haapalinna, S. Nevas, and D. Pähler, Rotational grinding of silicon wafers—sub-surface damage inspection, Mater. Sci. Eng. 107 (2004) 321-331.

DOI: 10.1016/j.mseb.2003.12.008

Google Scholar

[2] Y.Mizushima, Y.Kim, T.Nakamura, R.Sugie, H.Hashimoto, A.Uedono, & T. Ohba, Impact of back-grinding-induced damage on Si wafer thinning for three-dimensional integration, J. Appl. Phys. 53 (2014) 05GE04.

DOI: 10.7567/jjap.53.05ge04

Google Scholar

[3] H. Sako, H. Matsuhata, M. Sasaki, M. Nagaya, T. Kido, K. Kawata, T. Kato, J. Senzaki, M. Kitabatake, and H. Okumura, Micro-structural analysis of local damage introduced in subsurface regions of 4H-SiC wafers during chemo-mechanical polishing, J. Appl. Phys. 119 (2016) 135702.

DOI: 10.1063/1.4945017

Google Scholar

[4] K. Ashida, D. Dojima, Y. Kutsuma, S. Torimi, S. Nogami, Y. Imai, S. Kimura, J. Mizuki, N. Ohtani, and T. Kaneko, Evaluation of Polishing-Induced Subsurface Damage of 4H-SiC (0001) by Cross-Sectional Electron Backscattered Diffraction and Synchrotron X-Ray Micro-Diffraction, MRS Adv. 1 (2016) 3697-3702.

DOI: 10.1557/adv.2016.433

Google Scholar

[5] T. Höchbauer, C. Heidorn, and N. Tsavdaris, New SiC epitaxial growth process with up to 100% BPD to TED defect conversion on 150mm hot-wall CVD reactor, Mater. Sci. 963 (2019) 123-126

DOI: 10.4028/www.scientific.net/msf.963.123

Google Scholar

[6] K. Toda, D. Dojima, K. Kojima, H. Mihara, S. Mitani, and T. Kaneko, Suppression of In-Grown SF Formation and BPD Propagation in 4H-Sic Epitaxial Layer by Sublimating Sub-Surface Damage before the Growth, Solid State Phenom. 344 (2023) 9-14.

DOI: 10.4028/p-z108w8

Google Scholar

[7] D. Dojima, D. Dansako, M. Maki, K. Toda, and T. Kaneko, 4H-SiC Full Wafer Mapping Image of CMP-Finished Sub-Surface Damage by Laser Light Scattering, Solid State Phenom. 343 (2023) 43-50.

DOI: 10.4028/p-1i3w12

Google Scholar

[8] SG Sridhara, T.J. Eperjesi, R.P. Devaty, and W.J. Choyke, Penetration depths in the ultraviolet for 4H, 6H and 3C silicon carbide at seven common laser pumping wavelengths, Mater. Sci. Eng. 61-62 (1999) 229-233.

DOI: 10.1016/s0921-5107(98)00508-x

Google Scholar