Basal Plane Dislocation Analysis of 4H-SiC Using Multi Directional STEM Observation

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Abstract:

A peculiar surface defect on a silicon carbide (SiC) epitaxial wafer, found to be associated a basal plane dislocation (BPD), was studied using a low energy scanning electron microscope (LESEM), and a novel method we are calling multi directional scanning transmission electron microscopy (MD-STEM). We have confirmed that an etch pit with double cores neighboring a peculiar surface defect is derived from the extended BPD. The BPD consisted of two partial dislocations with a stacking fault width of about 100 nm. Observation of only one viewing direction in a previous study missed the extended dislocation but through the use of the MD-STEM method in the current study, the dislocation has been confirmed to be extended into a stacking fault.

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Materials Science Forum (Volumes 821-823)

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303-306

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June 2015

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© 2015 Trans Tech Publications Ltd. All Rights Reserved

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[1] T. Isshiki, Abs. 8th Japanese-Polish Joint seminar, Uji, Japan, 2010, pp.4-7.

Google Scholar

[2] T. Sato, Y. Suzuki, H. Ito, T. Isshiki and M. Fukui, Materials Science Forum Vols. 778-780 (2014) , pp.358-361.

DOI: 10.4028/www.scientific.net/msf.778-780.358

Google Scholar

[3] Y. Orai, S. Watanabe, T. Sato, T. Isshiki and M. Fukui, Proc. ECSCRM2014 Tu-P-35.

Google Scholar

[4] T. Kamino, T. Yaguchi, M. Konno, T. Ohnishi and T. Ishitani, Journal of Electron Microscopy 53(6), pp.583-588.

Google Scholar

[5] T. Ohnishi, H. Koike and T. Ishitani, Proc. 25th International Symposium for Testing and Failure Analysis 1999, pp.449-453.

Google Scholar

[6] T. Ohnishi and T. Ishitani, US patent 5270552 (1992).

Google Scholar